catena-Poly[[(dimethyl­formamide-κO)copper(II)]-bis­(μ-4-nitro­phenyl­cyanamido-κ2 N 1:N 3)]

نویسندگان

  • Hossein Chiniforoshan
  • Soghra Jalilpour
  • Bahare Shirinfar
  • Hamid Reza Khavasi
چکیده

In the title compound, [Cu(C(7)H(4)N(3)O(2))(2)(C(3)H(7)NO)], the Cu(II) atom is five-coordinated in a distorted square-pyramidal geometry, with the N atoms in equatorial positions and the dimethyl-formamide O atom in an axial position. The dihedral angle between adjacent benzene rings is 70.33 (12)°.

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catena-Poly[[bis­(dimethyl­formamide-κO)cadmium]-bis­(μ-4-nitro­phenyl­cyanamido-κ2 N 1:N 3)]

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A triclinic polymorph of catena-poly[[bis­(N,N-dimethyl­formamide-κO)cobalt(II)]-di-μ-1,5-dicyanamido-κ4 N 1:N 5]

The title compound, [Co(C(2)N(3))(2)(C(3)H(7)NO)(2)](n), is a triclinic polymorph of the previously reported monoclinic structure [Tong et al. (2003 ▶). Acta Cryst. E59, m405-m407]. The Co(II) ion lies on an inversion centre and adopts an almost regular octa-hedral N(4)O(2) coordination geometry. Adjacent Co(II) atoms are connected by two bridging dicyanamide ligands, resulting in the formation...

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عنوان ژورنال:

دوره 65  شماره 

صفحات  -

تاریخ انتشار 2009